The CIREM currently operates four high field NMR spectrometers for liquid measurements.
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JEOL JNM-ECZ400R/S3 spectrometerShielded 9.4 Tesla Superconducting Magnet (400 MHz)
2-channel console (high, low) with pulsed field gradient (PFG) and variable temperature (VT) units FTS air-cooling device and liquid-nitrogen boil-off cooling system Measurement temperature range: -100 °C to + 150°C 30-sample carousel for automation Probes: 1) 5 mm NM Royal probe with z-PFG and auto-tune for double resonance 31P-15N/1H-19F experiments 2) 5 mm NM Royal HFX probe with z-PFG and auto-tune for triple resonance 31P-15N/1H/19F experiments on two channels |
| JEOL JNM-ECZ600R/S3 spectrometer
Shielded 14.1 Tesla Superconducting Magnet (600 MHz) 3-channel console (high, high, low) with pulsed field gradient (PFG) and variable temperature (VT) units FTS air-cooling device and liquid-nitrogen boil-off cooling system Measurement temperature range: -100 °C to + 150°C 30-sample carousel for automation Probes: 1) 5 mm NM Royal probe with z-PFG and auto-tune for double resonance 31P-15N/1H-19F experiments 2) 10 mm low-gamma probe for double resonance 15N-103Rh/1H experiments Measurement temperatures : – 50 °C to + 120°C 3) 5 mm CFH probe with z-PFG for triple resonance 13C/19F/1H experiments |
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